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X-Band Metamaterial-Based Resonant Sensor for Food Quality Monitoring

Fahmiruddin Esa, Nurdiana Anis Ibrahim, Huda A Majid, Man Seng Sim, Kok Yeow You

Abstract


This paper presents a highly sensitive metamaterial-based resonant sensor operating at X-band for rapid and non-destructive monitoring of food quality. The sensor incorporates an I-beam and C-shaped resonator configuration, with quality assessment achieved through resonant frequency shift and resonance broadening, reflected in the quality factor (Q-factor). The structure was designed and optimized using Computer Simulation Technology (CST) Microwave Studio Suite and experimentally validated using a network analyzer with an X-band rectangular waveguide. The unloaded X-band waveguide-integrated resonator exhibited a high Q-factor of 36.463, suitable for powder characterization. For semi-liquid and liquid samples, a custom 3D-printed cuvette was introduced to improve handling and measurement stability, increasing the Q-factor to 43.498 due to higher moisture sensitivity. The sensor’s applicability was demonstrated on cooking powder, oil, and honey. It successfully differentiated soup powder and curry powder with a minimal moisture difference of 0.3%, where increasing moisture content reduced the Q-factor due to enhanced microwave absorption. For honey samples, the Q-factor showed strong correlation with sugar concentration, decreasing with higher glucose and fructose content as reduced free water and increased density altered dielectric properties. Viscosity trends reflect not only sugar concentration but also the influence of bioactive compounds such as polyphenols and flavonoids. In cooking oil analysis, the sensor clearly distinguished fresh and used oil through slight resonant frequency shifts and Q-factor variations, even when FTIR spectroscopy showed limited quantifiable color-related changes caused by oxidation and triglyceride polymerization. Rheological measurements indicated higher viscosity in fresh oil (2.2–2.7 mPa·s) compared to used oil (1.3–1.5 mPa·s), consistent with thermal degradation effects. Overall, the proposed metamaterial sensor demonstrates enhanced sensitivity, compactness, and versatility, confirming its strong potential for real-time industrial food quality monitoring.

Keywords



[1] M. V. Zambrano, B. Dutta, D. G. Mercer, H. L. MacLean, and M. F. Touchie, “Assessment of moisture content measurement methods of dried food products in small-scale operations in developing countries: A review,” Trends in Food Science & Technology, vol. 88, pp. 484–496, Jun. 2019. doi: 10.1016/j.tifs. 2019.04.006

[2] H. Niu, M. Zhang, D. Shen, A. S. Mujumdar, and Y. Ma, “Sensing materials for fresh food quality deterioration measurement: a review of research progress and application in supply chain,” Critical Reviews in Food Science and Nutrition, pp. 1–19, Apr. 2023. doi: 10. 1080/10408398. 2023.2195939

[3] R. T. Blakey and A. M. Morales-Partera, “Microwave dielectric spectroscopy – A versatile methodology for online, non-destructive food analysis, monitoring and process control,” Engineering in Agriculture, Environment and Food, vol. 9, no. 3, pp. 264–273, Jul. 2016.

[4] R. Raju, G. E. Bridges, and S. Bhadra, “Wireless passive sensors for food quality monitoring: Improving the safety of food products,” IEEE Antennas and Propagation Magazine, vol. 62, no. 5, pp. 76–89, Oct. 2020.

[5] N. Miura, S. Yagihara, and S. Mashimo, “Microwave dielectric properties of solid and liquid foods investigated by time-domain reflectometry,” Journal of Food Science, vol. 68, no. 4, pp. 1396–1403, May 2003, doi: 10.1111/j. 1365-2621.2003.tb09656.x

[6] E. Iaccheri, A. Berardinelli, G. Maggio, T. G. Toschi, and L. Ragni, “Affordable time-domain reflectometry system for rapid food analysis,” IEEE Transactions on Instrumentation and Measurement, vol. 70, pp. 1–7, 2021, doi: 10.1109/TIM.2021.3069050

[7] H. He et al., “A review of time domain reflectometry (TDR) applications in porous media,” Advances in Agronomy, pp. 83–155, 2021, doi: 10.1016/bs.agron.2021.02.003

[8] D. Prakash and N. Gupta, “Applications of metamaterial sensors: A review,” International Journal of Microwave and Wireless Technologies, vol. 14, no. 1, pp. 19–33, Feb. 2021, doi: 10.1017/ s1759078721000039

[9] N. Kazemi, M. Abdolrazzaghi, P. Musilek, and E. Baladi, “A planar compact absorber for microwave sensing based on transmission-line metamaterials,” IEEE Sensors Journal, pp. 1–1, Jan. 2024.

[10] R. Srivastava and S. N. Kale, “Metamaterial inspired resonators as microwave sensors: A review,” Engineering Science & Technology, pp. 28–47, Aug. 2023, doi: 10.37256/est.5120242960

[11] M. S. Sim et al., “Microwave sensors loaded with metamaterial-inspired resonators for dielectric material characterization: A review,” Sensors and Actuators A: Physical, vol. 372, p. 115322, Apr. 2024, doi: 10.1016/j.sna.2024.115 322

[12] Z. Meng, Z. Wu, and J. Gray, “Microwave sensor technologies for food evaluation and analysis: Methods, challenges and solutions,” Transactions of the Institute of Measurement and Control, vol. 40, no. 12, pp. 3433–3448, Sep. 2017, doi: 10.1177/ 0142331217721968

[13] Y. I. Abdulkarim et al., “Highly sensitive metamaterial-based microwave sensor for the application of milk and dairy products,” Applied Optics, vol. 61, no. 8, pp. 1972–1972, Feb. 2022, doi: 10.1364/AO.451900

[14] K. Karthikeyan, P. S. Praveen Anandh, M. Ramesh, and V. Saran, “Design and parameter optimization of microwave sensor for fat content detection in milk,” AIP Conference Proceedings, vol. 3232, pp. 030002–030002, Jan. 2024, doi: 10.1063/5.0236788.

[15] K. Brinker, M. Dvorsky, M. T. Al Qaseer, and R. Zoughi, “Review of advances in microwave and millimetre-wave NDT&E: principles and applications,” Philosophical Transactions of the Royal Society A: Mathematical, Physical and Engineering Sciences, vol. 378, no. 2182, p. 20190585, Sep. 2020, doi: 10.1098/rsta.2019. 0585

[16] M. S. Sim, K. Y. You, F. Esa, and Y. L. Chan, “Nanostructured Electromagnetic Metamaterials for Sensing Applications,” Advances in Chemical and Materials Engineering, pp. 141–164, 2021, doi: 10.4018/978-1-7998-5563-7.ch009.

[17] S. Shamim, A. S. M. Mohsin, M. M. Rahman, and M. Belal, “Recent advances in the metamaterial and metasurface-based biosensor in the gigahertz, terahertz, and optical frequency domains,” Heliyon, vol. 10, no. 13, pp. e33272–e33272, Jun. 2024. doi: 10.1016 /j.heliyon.2024. e33272

[18] N. Meyne, C. Cammin, and A. F. Jacob, “Accuracy enhancement of a split-ring resonator liquid sensor using dielectric resonator coupling,” in 2014 20th International Conference on Microwaves, Radar and Wireless Communications (MIKON), Gdansk, Poland: IEEE, Jun. 2014, pp. 1–4. doi: 10.1109/MIKON. 2014.6899869.

[19] M. H. Baharuddin, M. F. Jamlos, M. Jusoh, M. R. Kamarudin, M. F. Jamlos, and M. F. A. Malek, “A review of characterization techniques for material's properties measurement using microwave resonant sensor,” Journal of Telecommunication, Electronic and Computer Engineering, vol. 10, no. 1-9, pp. 57–61, 2018.

[20] K. Y. You and S. K. Goudos, “Materials characterization using microwave waveguide system,” in Microwave Systems and Applications, pp. 341–358, 2017, doi: 10.5772/ 66230

[21] T. Dahms, D. B. Hayman, B. Mohamadzade, and S. L. Smith, “Measurement of dielectric properties of thin materials for radomes using waveguide cavities,” Telecom, vol. 5, no. 3, pp. 706–722, Aug. 2024, doi: 10.3390/telecom 5030036.

[22] S. Harnsoongnoen, “Microwave sensors based on coplanar waveguide loaded with split ring resonators: A review,” Applied Science and Engineering Progress, vol. 12, no. 4, pp. 224–234, 2019. doi: 10.14416/j.ijast. 2018.11.006

[23] Md. Rashedul Islam et. al., “Metamaterial sensor based on reflected mirror rectangular split ring resonator for the application of microwave sensing,” Measurement, vol. 198, p. 111416, Jul. 2022. doi: 10.1016/j. measurement.2022.111416

[24] Y. Li et. al., “Dielectric properties of chili powder in the development of radio frequency and microwave pasteurisation,” International Journal of Food Properties, vol. 20, no. sup3, pp. S3373–S3384, Dec. 2017.

[25] S. Qi et al., “Dielectric properties of edible fungi powder related to radio-frequency and microwave drying,” Food production, processing and nutrition, vol. 3, no. 1, Jun. 2021.

[26] L. C. Costa, S. S. Teixeira, and F. Henry, “Measuring microwave dielectric properties of materials: Theory and applications,” Materials Research Bulletin, vol. 179, Art. no. 112976, 2024, doi: 10.1016/j.materresbull. 2024.112976.

[27] A. Alimenti, K. Torokhtii, P. Vidal García, N. Pompeo, and E. Silva, “Design and test of a new dielectric-loaded resonator for the accurate characterization of conductive and dielectric materials,” Sensors, vol. 23, no. 1, Art. no. 518, 2023, doi: 10.3390/s23010518.

[28] Z. Li, Z. Meng, A. Haigh, P. Wang, and A. Gibson, “Characterisation of water in honey using a microwave cylindrical cavity resonator sensor,” Journal of Food Engineering, vol. 292, pp. 110373–110373, Mar. 2021. doi: 10.1016/j. jfoodeng.2020.110373

[29] Q. Jin, Z. Meng, Z. Chen, and Z. Li, “Review of scientific instruments: Evaluation of adulteration in honey using a microwave planar resonator sensor,” Review of Scientific Instruments, vol. 94, no. 10, Oct. 2023, doi: 10.1063/5.0166005

[30] I. Singh and S. Singh, “Honey moisture reduction and its quality,” Journal of Food Science and Technology, vol. 55, no. 10, pp. 3861–3871, 2018, doi: 10.1007/s13197-018-3341-5

[31] W. Guo, X. Zhu, Y. Liu, and H. Zhuang, “Sugar and water contents of honey with dielectric property sensing,” Journal of Food Engineering, vol. 97, no. 2, pp. 275–281, Mar. 2010, doi : 10.1016/j.jfoodeng.2009.10.024

[32] K. Polatidou, C. Nouska, C. Tananaki, C. G. Biliaderis, and A. Lazaridou, “ Physicochemical and rheological characteristics of monofloral honeys—kinetics of creaming–crystallization,” Foods, vol. 14, no. 10, pp. 1835 May 2025, doi:10.3390/foods14101835

[33] T. Castillo Martínez, C. García Osorio, J. G. García Muñiz, J. Aguilar Ávila, & R. Ramírez Valverde, “Sugars and °Brix in honey from Apis mellifera, Melipona beecheii, and commercial honey from a local market in Mexico,” Veterinaria México OA, vol. 9, Sep. 2022, doi:10.22201/fmvz.24486760e.2022.950.

[34] M. Sahlan, S. Karwita, M. Gozan, H. Hermansyah, M. Yohda, Y. J. Yoo, & D. K. Pratami, “Identification and classification of honey’s authenticity by attenuated total reflectance Fourier-transform infrared spectroscopy and chemometric method,” Veterinary World, vol. 12, no. 8, pp. 1304–1310, Aug. 2019, doi:10.14202/vetworld. 2019.1304-1310.

[35] N. D. Rodrigues, S. C. Palomares, and E.-R. E. Mojica, “Multivariate analysis of the ATR-FTIR of honey samples,” Journal of Undergraduate Chemistry Research, vol. 24, no. 1, pp. 33–37, Feb. 2025.

[36] O. Escuredo, I. Dobre, M. Fernández-González, and M. C. Seijo, “Contribution of botanical origin and sugar composition of honeys on the crystallization phenomenon,” Food Chemistry, vol. 149, pp. 84–90, Apr. 2014. doi : 10.1016/ j.foodchem.2013.10.097

[37] M. A. Al-Kafaween, M. Alwahsh, A. B. Mohd Hilmi, and D. H. Abulebdah, “Physicochemical characteristics and bioactive compounds of different types of honey and their biological and therapeutic properties: A comprehensive review,” Antibiotics, vol. 12, no. 2, Art. 337, 2023, doi: 10.3390/antibiotics12020337

[38] P. M. da Silva, C. Gauche, L. V. Gonzaga, A. C. O. Costa, and R. Fett, “Honey: Chemical composition, stability and authenticity,” Food Chemistry, vol. 196, pp. 309–323, Apr. 2016, doi: 10.1016/j.foodchem.2015.09.051.

[39] S. Yahya, F. H. Razali, and F. W. Harun, “Physicochemical properties of refined palm cooking oil and used palm cooking oil,” Materials Today: Proceedings, vol. 19, pp. 1166–1172, 2019, doi: 10.1016/j.matpr.2019. 11.010

[40] P. S. Dewi and M. Ulfah, “Quality test of palm cooking oil used repeatedly based on free fatty acid content, moisture content, peroxide number,” Journal of Science and Technology Research for Pharmacy, vol. 1, no. 1, pp. 34–41, Mar. 2021. doi: 10.15294/jstrp. v1i1.44461

[41] A. A. A. Wahab, S. H. Chang, and A. M. Som, “Characterization of waste cooking oil as a potential green solvent for liquid-liquid extraction,” Proceedings of the International Conference on Advances in Civil and Environmental Engineering (ACEE 2015), Penang, Malaysia, 2015, doi: 10. 1371/journal. pone.0232997

[42] S. M. Alshuiael and M. Al-Ghouti, “Multivariate analysis for FTIR in understanding treatment of used cooking oil using activated carbon prepared from olive stone,” PLoS ONE, vol. 15, no. 5, May 2020, doi: 10.1371/journal.pone.0232997

[43] M. M. Hassanein, S. M. El-Shami, and M. Hassan El-Mallah, “Changes occurring in vegetable oils composition due to microwave heating,” Grasas aceites, vol. 54, no. 4, pp. 343–349, Dec. 2003, doi : 10.3989/ gya.2003.v54.i4. 219

[44] X. Chen and S. Sun, “Color reversion of refined vegetable oils: A review,” Molecules, vol. 28, no. 13, Art. 5177, 2023, doi : 10.3390/molecules 28135177

[45] Q. Li et al., “ Indication of the color change on the oxidation properties of fragrant rapeseed oil during shelf storage,” Food Chemistry: X, vol. 20, art. no. 100908, 2023, doi: 10.1016/j.fochx. 2023.100908.

[46] S. N. Sahasrabudhe, J. A. Staton, and B. E. Farkas, “Effect of frying oil degradation on surface tension and wettability,” LWT, vol. 99, pp. 519–524, Jan. 2019. doi: 10.1016/j.lwt. 2018.10.026

[47] L. Cui, J. Chen, J. Zhai, L. Peng, and D. Hayes, “ Oil penetration of batter-breaded fish nuggets during deep-fat frying: effect of frying oils,” Foods, vol. 11, no. 21, pp. 3369, Oct. 2022. doi : 10.3390/foods11213369

[48] B. Wiege, E. Fehling, B. Matthäus, and M. Schmidt, “ Changes in physical and chemical properties of thermally and oxidatively degraded sunflower oil and palm fat,” Foods, vol. 9, no. 9, pp. 1273, Sep. 2020. doi : 10.3390/foods 9091273

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DOI: 10.14416/j.asep.2026.06.011

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